Powder metallurgy

We are active in the field of powder metallurgy in the area of obtaining advanced engineering and functional materials by sintering powders of metals, ceramics, metal matrix composites (MMCs), ceramic matrix composites (CMCs), nanolaminar multilayer carbides (MAX phases), and poorly sinterable materials using the FAST/SPS method. We conduct high-energy ball milling and mechanical synthesis of powders in a protective atmosphere with temperature and pressure control. Qualitative and quantitative studies of powders, bulk materials and thin coatings are carried out by X-ray diffraction XRD and GIXRD, thanks to access to the full ICDD PDF-4+ database.

Our products are used in the space industry, as well as in bioengineering or batteries. They are used to protect surfaces from corrosion or temperature.

Manufacture of materials by spark-plasma sintering technology
  • The spark-plasma sintering method allows sintering under high temperature and high pressure conditions. This offers the possibility of non-stoichiometric synthesis and obtaining solid sinters.
  • Rapid manufacturing of innovative materials difficult or impossible to obtain with traditional technologies
  • Possibility of sintering materials with melting points above 3000°C in up to tens of minutes (from powder to finished sinter).

We have the largest SPS device in Poland

Parameter

Sintering temperature

Pressing force

Heating rate

Sinter diameter

Atmosphere

Value

up to 2200°C

up to 250 kN

up to 1000°C/min

up to80 mm

Ar, N2, H2, vacuum

Urządzenie do iskrowego spiekania plazmowego proszków SPS HP D 25

HP D 25/3

High Energy Ball Milling (HEBM)

Powder preparation is a very important step in sintering or spraying processes. In our typical studies, we use high-energy ball milling and mechanical synthesis of powders. A specialist can control the temperature and pressure during the milling process. Phase transformations can be controlled by X-ray diffractometry.

Parameter

Rotation speed

Material of milling vessels and bowls

Maximum milling vessel capacity

Milling atmosphere

Value

up to 500 rpm

WC-Co, ZrO2, stainless steel

250 ml

Ar, N2, He, air

Młynek planetarno-kulowy Pulverisette 5 stosowany do mechanicznej syntezy i wysokoenergetycznego mielenia proszków
What else does powder metallurgy offer include?
  • Annealing in a protective or reducing atmosphere,
  • Vacuum drying,
  • Phase composition studies (qualitative and quantitative) by X-ray diffraction (XRD and GIXRD),
  • Spark plasma sintering / SPS, Spraying,
  • Vacuum cold spraying / VCS, Aerosol Cold Spray / ACS,
  • MAX phases, cemented carbides, composite materials, qualitative and quantitative phase analysis by X-ray diffraction (XRD), mechanical synthesis.

Our experts will prepare a favourable proposal for you.

    Our expert:

    Maria Wiśniewska

    Phone: +48 61 657 05 55

    Sieć Badawcza Łukasiewicz – Poznański Instytut Technologiczny, Centrum Zrównoważonej Gospodarki, ul. Jana Pawła II 14, 61 – 139 Poznań

    Maria Wiśniewska, ekspertka Łukasiewicz - PIT w dziedzinie metalurgii proszków